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dc.contributor.authorAydoǧan, C. and Denizli, A.
dc.date.accessioned2021-04-08T12:09:29Z
dc.date.available2021-04-08T12:09:29Z
dc.date.issued2014
dc.identifier10.1016/j.ab.2013.11.006
dc.identifier.issn00032697
dc.identifier.urihttps://www.scopus.com/inward/record.uri?eid=2-s2.0-84891368607&doi=10.1016%2fj.ab.2013.11.006&partnerID=40&md5=68a0d016401098ed316bfa55cbf88da3
dc.identifier.urihttp://acikerisim.bingol.edu.tr/handle/20.500.12898/4841
dc.description.abstractChiral ligand-exchange enantioseparation of aliphatic and aromatic amino acids was successfully performed using a new open-tubular zwitterionic column with tentacle-type polymer stationary phase. The polymeric stationary phase was prepared using 3-chloro-2-hydroxypropyl methacrylate (HPMA-Cl), a new reactive monomer. The preparation procedure of the open-tubular column included silanization, in situ graft polymerization with HPMA-Cl, and l-histidine (l-His) modification. l-His was used as a chiral ligand-exchange selector and copper(II) as a central ion. Successful enantioseparation of six pairs of amino acid enantiomers was achieved with a buffer of 5 mM CuSO4, 20 mM (NH4)2SO4 at pH 3.0. © 2013 Elsevier Inc. All rights reserved.
dc.language.isoEnglish
dc.sourceAnalytical Biochemistry
dc.titleChiral separation-based ligand exchange by open-tubular capillary electrochromatography


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